Name of the equipment: High Resolution Mass Spectrometer with LC (LC-HRMS) Make & Model: Waters, Synapt XS with Aquity H class UPLC I-Stem Registration ID- 3244309 Category of Instrument Mass spectrometry Types of Analysis / Testing Characterisation & Testing Application: Determination of elemental composition, quantitation, identification of unknown compounds, measuring the exact mass of the compounds. Description of Instrument HRMS offers both high resolution & high mass accuracy and is a powerful tool for the analysis & quantitation of compounds.
Book through I-STEM: https://www.istem.gov.in/ Slot Booking Link I-STEM Slot Booking link for External User	Booking available for Internal and External Both Requisition form for Internals Externals

Faculty In-charge: Dr. Anuj A Vargeese Email ID: aav@nitc.ac.in Phone number:   +91-9700455320	Technical Staff: Ruther Tyson Lewis Email ID: ruthertl@nitc.ac.in Phone number: 9845965130	Department Chemistry Office Email ID: chyoffice@nitc.ac.in Location Sophisticated Instruments Lab                Dept. of Chemistry

Instrument Technical Description · ToF Resolution +^ve & -^ve ion: 75,000 FWHM. · Mass range : 100-64,000 m/z (V mode)                     : 100-16,000 m/z (W mode) · +^veion sensitivity: 50pg/µL leucin enkephalin · +^veion MS/MS sensitivity: 100fmol/µL Fibrinopeptide · -^ve ion MS sensitivity: 50pg/µL leucin enkephalin · -^ve ion MS/MS sensitivity: 500pg/ µL raffinose. · Dynamic range: 4 orders. · Mass measurement accuracy: <1ppm

Features of the equipment ● Lock spray mass technology for measuring exact mass. ● Unispray Ion Source. ● Electron transfer dissociation & collision Induced dissociation fragmentation for providing accurate MS/MS data. ● The StepWave XS ion guide removes neutral species & transmits ions in a more focused beam to the detector

· Quantity: 3-5 mg

· Sample Type: Solid & Liquid.

· The sample has to be soluble in one of the four solvents (water, methanol, acetonitrile & iso propyl alcohol).

· The User should reveal the toxicity/ hazardous nature of the sample in the requisition form.

· Minimum No. of Days Required for Analysis: 1 week

	Liquid/Solid (Analysis: HRMS) (charges per 1 sample)	Liquid/Solid (Analysis: LC-HRMS) (charges per 1 sample)	Liquid/Solid (Analysis: MS/MS) (charges per 1 sample)
NIT Calicut User	Rs. 100/-	Rs. 200/-	Rs.50/- (each ion in addition to the HRMS/LC-HRMS)
External Academia Research institute User	Rs. 500/-	Rs. 1000/-	Rs.250/- (each ion in addition to the HRMS/ LC-HRMS)
National lab User	Rs. 600/-	Rs. 1200/-	Rs.350/- (each ion in addition to the HRMS/ LC-HRMS)
Industry User	Rs. 1000/-	Rs. 1750/-	Rs.500/- (each ion in addition to the HRMS/ LC-HRMS)